Standard Procedure For Determination of Softening Point of Bitumen
References: AASHTO 53-96
ASTM 36-93
Definitions:
Instruments:
1. Rings
2. pouring Plate
3.Bath
4. Balls
5.Centering Guide
6. Ring and ball Holder
7.Thermometer
Sampling:
For Taking sample for this test is simply follow the instruction described in
Sampling Page.
Test Specimens Notes:
- Be sure to start the test just after complete preparation of all
equipments and sample
- Do not heat the sample for more than 2 hours
- If the test rejected sampling rejected and or repeating the test required
,Do not use the Heated sample again.
Procedure:
- Put the sample in oven to get heated ,get (prepare) fresh and if possible
distilled water for test, Which has the temperature of 30-80 C ,But the
starting point for test is 5°±1 C.
- Pour the heated sample into rings and let them to be cool in normal air
temperature. after cooling period cut (clean) the extra sample from the top of
the rings by using a heated spatula or ant other sharp device , be care full
to do not dig the entire filled sample from the ring.
- fill up the glass from water ,be sure that the depth of the water in bath
must be at least 105 mm (including the placed instrument into water during the
filling up the bath).
- Put the bath into water or add ice into water if necessary ,put the ring
in ring holder and put the balls on top of the rings. install the thermometer
.
- let the bath temperature get down to desired temperature( 5°±1°),after
reaching the goal temperature, start the heating from the bottom of the bath
,whit rate of 5°c /minute, Do not
average the rate, be sure that the Total change in rate be less than
0.5°C, other wise the test will be reject.
- Record the time of completely fall down of ball and reach to the surface
of the holder for each ball.
- It is important to know that the result of the test using fresh water and
using water and glycerin solution is deferent ,but the most useful method here
is using the water and ignore other possibility for this test.